(1)電子天平
電(dian)子(zi)天(tian)平(ping)是(shi)我(wo)們(men)的(de)化(hua)學(xue)實(shi)驗(yan)中(zhong)必(bi)備(bei)的(de)稱(cheng)量(liang)工(gong)具(ju),學(xue)生(sheng)也(ye)基(ji)本(ben)能(neng)掌(zhang)握(wo)其(qi)使(shi)用(yong)方(fang)法(fa),但(dan)實(shi)驗(yan)的(de)細(xi)節(jie)和(he)打(da)掃(sao)維(wei)護(hu)做(zuo)的(de)很(hen)不(bu)到(dao)位(wei),實(shi)驗(yan)後(hou)秤(cheng)盤(pan)下(xia)殘(can)留(liu)有(you)一(yi)些(xie)物(wu)質(zhi),秤(cheng)盤(pan)上(shang)留(liu)有(you)汙(wu)漬(zi)。使(shi)天(tian)平(ping)的(de)靈(ling)敏(min)度(du)和(he)準(zhun)確(que)度(du)下(xia)降(jiang),使(shi)用(yong)壽(shou)命(ming)也(ye)縮(suo)短(duan)。電(dian)子(zi)天(tian)平(ping)使(shi)用(yong)前(qian)須(xu)先(xian)預(yu)熱(re)10分fen鍾zhong,但dan部bu分fen學xue生sheng開kai機ji後hou直zhi接jie稱cheng量liang。稱cheng量liang物wu的de溫wen度du必bi須xu與yu天tian平ping溫wen度du相xiang同tong,不bu能neng把ba過guo熱re或huo過guo冷leng的de物wu體ti放fang在zai天tian平ping秤cheng盤pan上shang。一yi些xie具ju有you揮hui發fa性xing的de腐fu蝕shi性xing的de試shi劑ji應ying放fang在zai密mi閉bi容rong器qi中zhong稱cheng量liang,稱cheng量liang物wu體ti時shi要yao切qie記ji關guan閉bi天tian平ping的de側ce門men,稱cheng量liang完wan畢bi後hou及ji時shi打da掃sao稱cheng量liang盤pan上shang下xia及ji各ge個ge角jiao落luo等deng。在zai空kong氣qi潮chao濕shi,物wu質zhi已yi結jie成cheng垢gou塊kuai時shi,應ying采cai用yong機ji械xie除chu鏽xiu方fang法fa,即ji先xian用yong鏟chan、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。
(2)電熱恒溫幹燥箱
電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100-110du,buyiguogao。keranxinghehuifaxingdehuaxuewupinqiewufangruxiangnei,xiangneizaiwuyingbaifangyingzaigebandejiaozhongxinbuwei,tongshibuyingxiangkongqiliutongyibaozhengxiangneiwendujunyun。ganzaoxiangshiyongguochengzhong,xueshengbunengyongshishouchumoxiangtihekaiguan。ganzaoxiangzhengchangyunxingshiruzaishiyongguochengzhongchuxianyichang、氣味、煙(yan)霧(wu)等(deng)情(qing)況(kuang),應(ying)立(li)即(ji)關(guan)閉(bi)電(dian)源(yuan),請(qing)專(zhuan)業(ye)人(ren)員(yuan)查(zha)看(kan)修(xiu)理(li)。箱(xiang)壁(bi)內(nei)膽(dan)和(he)設(she)備(bei)表(biao)麵(mian)要(yao)經(jing)常(chang)擦(ca)拭(shi),以(yi)保(bao)持(chi)清(qing)潔(jie),增(zeng)加(jia)玻(bo)璃(li)的(de)透(tou)明(ming)度(du)。幹(gan)燥(zao)箱(xiang)若(ruo)長(chang)期(qi)不(bu)用(yong),應(ying)拔(ba)掉(diao)電(dian)源(yuan)線(xian)以(yi)防(fang)止(zhi)設(she)備(bei)損(sun)傷(shang)人(ren),並(bing)應(ying)定(ding)期(qi)按(an)使(shi)用(yong)條(tiao)件(jian)運(yun)行(xing)2-3天,以驅除電器部分的潮氣,避免損壞有關器件。
(3)恒溫水浴鍋
恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、jiaoyukeyandebibeigongju。zaishiyongzhongxueshengyinggaizhidaotadeshiyongfangfajizhuyishixiang,yibianshiyannenggoushunlijinxing。jiashuizhiqianqiewujietongdianyuan,zuihaojiaruzhengliushui,yimianchanshengshuigou,jiashuibuyaotaiduo,yimianfeitengshishuiliangyichuguowai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;切qie勿wu無wu水shui或huo水shui位wei低di於yu隔ge板ban加jia熱re,否fou則ze會hui損sun壞huai加jia熱re管guan。注zhu水shui時shi不bu能neng將jiang水shui流liu入ru控kong製zhi箱xiang內nei,以yi防fang發fa生sheng觸chu電dian。如ru恒heng溫wen控kong製zhi失shi靈ling,可ke將jiang控kong製zhi器qi上shang的de銀yin接jie點dian用yong細xi砂sha布bu擦ca亮liang。使shi用yong完wan畢bi後hou,取qu出chu恒heng溫wen物wu,關guan閉bi電dian源yuan,排pai除chu箱xiang體ti內nei的de水shui,做zuo好hao儀yi器qi使shi用yong記ji錄lu。
(1)燒杯
燒杯因其口徑上下一致,是取用液體、配製溶液、做zuo簡jian單dan化hua學xue反fan應ying最zui常chang用yong的de反fan應ying容rong器qi。但dan燒shao杯bei不bu能neng代dai替ti量liang筒tong量liang取qu液ye體ti。燒shao杯bei加jia熱re時shi要yao墊dian上shang石shi棉mian網wang。不bu能neng用yong火huo焰yan直zhi接jie加jia熱re燒shao杯bei。因yin為wei燒shao杯bei底di麵mian大da,用yong火huo焰yan直zhi接jie加jia熱re,隻zhi可ke燒shao到dao局ju部bu,使shi玻bo璃li受shou熱re不bu勻yun而er引yin起qi炸zha裂lie。用yong燒shao杯bei加jia熱re液ye體ti時shi,液ye體ti的de量liang以yi不bu超chao過guo燒shao杯bei容rong積ji的de1/3為wei宜yi,以yi防fang沸fei騰teng時shi液ye體ti外wai溢yi。加jia熱re時shi,燒shao杯bei外wai壁bi須xu擦ca幹gan。加jia熱re腐fu蝕shi性xing藥yao品pin時shi,可ke將jiang一yi表biao麵mian皿min蓋gai在zai燒shao杯bei口kou上shang,以yi免mian液ye體ti濺jian出chu。不bu可ke用yong燒shao杯bei長chang期qi盛sheng放fang化hua學xue藥yao品pin,以yi免mian落luo入ru塵chen土tu和he使shi溶rong液ye中zhong的de水shui分fen蒸zheng發fa。溶rong解jie或huo稀xi釋shi過guo程cheng中zhong,用yong玻bo璃li棒bang攪jiao拌ban時shi,不bu要yao觸chu及ji杯bei底di或huo杯bei壁bi。
(2)試管
實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。加jia熱re時shi要yao保bao持chi試shi管guan外wai壁bi沒mei有you水shui珠zhu,防fang止zhi受shou熱re不bu均jun勻yun而er爆bao裂lie。加jia熱re後hou不bu能neng驟zhou冷leng,防fang止zhi試shi管guan破po裂lie。加jia熱re後hou不bu能neng在zai試shi管guan未wei冷leng卻que至zhi室shi溫wen時shi就jiu洗xi滌di試shi管guan。加jia熱re時shi應ying用yong外wai焰yan。
(3)容量瓶
容rong量liang瓶ping主zhu要yao用yong於yu準zhun確que地di配pei製zhi一yi定ding摩mo爾er濃nong度du的de溶rong液ye,它ta是shi一yi種zhong細xi長chang頸jing,梨li形xing的de平ping底di玻bo璃li瓶ping,帶dai有you磨mo口kou玻bo璃li塞sai,瓶ping頸jing上shang刻ke有you標biao線xian,當dang瓶ping內nei液ye體ti在zai所suo指zhi定ding溫wen度du下xia達da到dao標biao線xian處chu時shi,其qi體ti積ji即ji為wei瓶ping上shang所suo注zhu明ming的de容rong積ji數shu。容rong量liang瓶ping不bu能neng配pei製zhi其qi容rong積ji以yi下xia體ti積ji的de溶rong液ye,即ji其qi容rong積ji為wei多duo大da,就jiu隻zhi能neng配pei製zhi多duo大da體ti積ji的de溶rong液ye。容rong量liang瓶ping使shi用yong前qian應ying先xian檢jian查zha是shi否fou漏lou水shui,依yi次ci用yong自zi來lai水shui,蒸zheng餾liu水shui洗xi好hao備bei用yong。將jiang溶rong質zhi在zai燒shao杯bei中zhong溶rong解jie後hou轉zhuan移yi到dao容rong量liang瓶ping裏li,不bu能neng在zai容rong量liang瓶ping裏li進jin行xing溶rong質zhi的de溶rong解jie,控kong製zhi溶rong解jie溶rong質zhi的de蒸zheng餾liu水shui量liang。轉zhuan移yi時shi必bi須xu用yong玻bo璃li棒bang引yin流liu。容rong量liang瓶ping不bu能neng進jin行xing加jia熱re,如ru果guo溶rong質zhi在zai溶rong解jie過guo程cheng中zhong放fang熱re,要yao待dai溶rong液ye冷leng卻que後hou再zai進jin行xing轉zhuan移yi,因yin為wei溫wen度du升sheng高gao瓶ping體ti將jiang膨peng脹zhang,所suo量liang體ti積ji就jiu會hui不bu準zhun確que。用yong於yu洗xi滌di燒shao杯bei的de溶rong劑ji總zong量liang不bu能neng超chao過guo容rong量liang瓶ping的de標biao線xian,一yi旦dan超chao過guo,必bi須xu重zhong新xin進jin行xing配pei置zhi。配pei製zhi好hao的de溶rong液ye轉zhuan移yi至zhi試shi劑ji瓶ping中zhong保bao存cun,容rong量liang瓶ping隻zhi能neng配pei製zhi溶rong液ye,不bu能neng儲chu存cun溶rong液ye,因yin為wei溶rong液ye可ke能neng會hui對dui瓶ping體ti進jin行xing腐fu蝕shi,從cong而er使shi容rong量liang瓶ping的de精jing度du受shou到dao影ying響xiang。容rong量liang瓶ping使shi用yong完wan畢bi應ying及ji時shi用yong水shui衝chong洗xi幹gan淨jing,塞sai上shang瓶ping塞sai,並bing在zai塞sai子zi與yu瓶ping口kou之zhi間jian夾jia一yi條tiao紙zhi條tiao,防fang止zhi瓶ping塞sai與yu瓶ping口kou粘zhan連lian。最zui後hou記ji錄lu溶rong液ye體ti積ji的de時shi候hou一yi般ban保bao留liu4位有效數字(XXX.0mL)。
(4)滴定管
滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水shui依yi次ci衝chong洗xi幹gan淨jing,並bing要yao用yong待dai裝zhuang的de溶rong液ye潤run洗xi滴di定ding管guan。將jiang操cao作zuo溶rong液ye倒dao入ru,直zhi到dao充chong滿man至zhi零ling刻ke度du線xian以yi上shang為wei止zhi。注zhu意yi檢jian查zha滴di定ding管guan的de出chu口kou管guan是shi否fou充chong滿man溶rong液ye,如ru有you氣qi泡pao進jin行xing排pai氣qi泡pao操cao作zuo。調tiao整zheng液ye麵mian時shi,使shi液ye麵mian保bao持chi在zai“0”或“0”以(yi)下(xia)的(de)某(mou)一(yi)定(ding)刻(ke)度(du)。進(jin)行(xing)滴(di)定(ding)時(shi),應(ying)將(jiang)滴(di)定(ding)管(guan)垂(chui)直(zhi)地(di)夾(jia)在(zai)滴(di)定(ding)管(guan)夾(jia)上(shang),如(ru)使(shi)用(yong)的(de)是(shi)堿(jian)式(shi)滴(di)定(ding)管(guan),拇(mu)指(zhi)與(yu)食(shi)指(zhi)在(zai)玻(bo)璃(li)珠(zhu)所(suo)在(zai)部(bu)位(wei)一(yi)旁(pang)捏(nie)乳(ru)膠(jiao)管(guan),不(bu)要(yao)捏(nie)玻(bo)璃(li)珠(zhu),也(ye)不(bu)能(neng)使(shi)其(qi)上(shang)下(xia)移(yi)動(dong)。滴(di)定(ding)時(shi)應(ying)逐(zhu)滴(di)連(lian)續(xu)滴(di)加(jia),接(jie)近(jin)終(zhong)點(dian)時(shi),隻(zhi)加(jia)一(yi)滴(di)或(huo)半(ban)滴(di),至(zhi)溶(rong)液(ye)出(chu)現(xian)明(ming)顯(xian)的(de)顏(yan)色(se)變(bian)化(hua)。讀(du)數(shu)時(shi),手(shou)拿(na)滴(di)定(ding)管(guan)上(shang)部(bu)無(wu)刻(ke)度(du)處(chu),使(shi)滴(di)定(ding)管(guan)保(bao)持(chi)垂(chui)直(zhi),視(shi)線(xian)平(ping)視(shi)溶(rong)液(ye)的(de)凹(ao)液(ye)麵(mian),讀(du)到(dao)小(xiao)數(shu)點(dian)後(hou)第(di)二(er)位(wei),即(ji)估(gu)計(ji)到(dao)0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。
附(fu)有(you)易(yi)去(qu)除(chu)物(wu)質(zhi)的(de)簡(jian)單(dan)儀(yi)器(qi),如(ru)試(shi)管(guan)。燒(shao)杯(bei)等(deng),先(xian)用(yong)自(zi)來(lai)水(shui)衝(chong)洗(xi),再(zai)用(yong)試(shi)管(guan)刷(shua)蘸(zhan)取(qu)合(he)成(cheng)洗(xi)滌(di)劑(ji)刷(shua)洗(xi),最(zui)後(hou)自(zi)來(lai)水(shui)衝(chong)洗(xi)。當(dang)倒(dao)置(zhi)儀(yi)器(qi),器(qi)壁(bi)形(xing)成(cheng)一(yi)層(ceng)均(jun)勻(yun)的(de)水(shui)膜(mo),不(bu)成(cheng)股(gu)流(liu)下(xia)時(shi),即(ji)已(yi)洗(xi)淨(jing)。
有油汙的玻璃器皿,先用堿性酒精洗滌液洗滌,然後用洗衣粉水或肥皂水洗滌,再用自來水衝洗幹淨。
有鏽跡,水垢的器皿,用(1+3)鹽酸洗液浸泡,再用再來水衝洗幹淨。
有凡士林油汙的器皿,先將凡士林擦去,再用洗衣粉水或肥皂水洗燒煮,取出後用自來水衝洗幹淨。
一些構造比較精細、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。
洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。
實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、pengzhuangyiqi,yifangzhiguangxuelingjiansunshangjiyingxiangjingdu。beiceshiyangzhongbuyingyouyingxingzazhi,dangceshigutishiyangshi,yingfangzhibazheshelengjingbiaomianlamaohuochanshengyahen。shiyongwanbihou,yanjinzhijiefangrushuizhongqingxi,bimianguangxuexitongguanlujinshui。dakailengjing,yongcajingzhiqingqingcagan,bulunzairenheqingkuangxia,buyunxuyongcajingzhiyiwaiderenhedongxijiechudaolengjing,yimiansunhuaitadeguangxuepingmian。yiqiyingcunfangyuganzao、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。
光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、xianweijingdejingtou,xianyongzhengliushuijinxingqingxi,jingmianruoyouwuzi,keyiyongyichunheyimidehunheyeqingxi。qingxishiyongzhuanmendecajingzhihuomianqiuzhanyoushaoliangqingxiji,shunzheyigefangxiangcashi,congjingtouzhongxinxiangwaizuoyuanyundong,qiejibazheleijingtoujinpaozaiqingxijizhongqingxi。qingxijingtoubudeyonglishica,fouzehuihuashangzengtoumo,sunhuaijingtou。qingxiwanbihouyongcajingzhicagan,biguangbaocun。
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