有的用戶如果對微量元素分析儀的專業知識缺乏或了解甚少,不要擔心,隻要掌握以下幾個要點,便可輕鬆應對。
第(di)一(yi)是(shi)重(zhong)複(fu)性(xing)穩(wen)定(ding)性(xing),這(zhe)是(shi)儀(yi)器(qi)最(zui)基(ji)本(ben)的(de)要(yao)求(qiu),是(shi)分(fen)析(xi)檢(jian)驗(yan)的(de)基(ji)礎(chu)。這(zhe)項(xiang)指(zhi)標(biao)不(bu)好(hao),其(qi)他(ta)就(jiu)無(wu)從(cong)談(tan)起(qi),純(chun)粹(cui)是(shi)忽(hu)悠(you)了(le)。如(ru)果(guo)同(tong)一(yi)個(ge)樣(yang)品(pin),檢(jian)測(ce)獲(huo)得(de)結(jie)果(guo)忽(hu)高(gao)忽(hu)低(di),相(xiang)差(cha)很(hen)大(da),這(zhe)說(shuo)明(ming)儀(yi)器(qi)有(you)問(wen)題(ti)。如(ru)果(guo)你(ni)看(kan)儀(yi)器(qi)實(shi)測(ce),一(yi)些(xie)廠(chang)家(jia)為(wei)避(bi)免(mian)方(fang)便(bian)地(di)觀(guan)測(ce)重(zhong)複(fu)性(xing),不(bu)讓(rang)操(cao)作(zuo)者(zhe)能(neng)方(fang)便(bian)地(di)迭(die)加(jia)曲(qu)線(xian),不(bu)設(she)置(zhi)求(qiu)變(bian)異(yi)係(xi)數(shu)的(de)程(cheng)序(xu),這(zhe)就(jiu)是(shi)因(yin)為(wei)儀(yi)器(qi)的(de)性(xing)能(neng)不(bu)佳(jia),怕(pa)被(bei)別(bie)人(ren)一(yi)眼(yan)看(kan)出(chu)問(wen)題(ti),生(sheng)產(chan)商(shang)在(zai)回(hui)避(bi)這(zhe)個(ge)問(wen)題(ti)。實(shi)際(ji)上(shang)一(yi)些(xie)廠(chang)家(jia)的(de)儀(yi)器(qi)變(bian)異(yi)係(xi)數(shu)在(zai)10—20%之間,誤差大大超過了有關規定,這樣做出的結果可信度低,我公司產品的變異係數內控在5%以下,通過儀器的測試可一目了然。
電化學中極譜分析使用的電極極小(指滴汞電),而靈敏度與電極比表麵積有關,麵積大信噪比高(指信號與噪聲的比值),靈ling敏min度du高gao,抗kang幹gan擾rao能neng力li強qiang,但dan由you於yu滴di汞gong電dian極ji麵mian積ji取qu決jue於yu體ti積ji,大da了le就jiu要yao不bu受shou控kong的de脫tuo落luo,因yin此ci電dian極ji表biao麵mian積ji受shou到dao嚴yan重zhong製zhi約yue,這zhe決jue定ding了le常chang規gui方fang式shi電dian極ji所suo做zuo的de儀yi器qi噪zao聲sheng大da,重zhong複fu性xing不bu佳jia,這zhe是shi目mu前qian所suo有you使shi用yong這zhe類lei電dian極ji儀yi器qi一yi個ge通tong病bing。隻zhi有you我wo公gong司si的de產chan品pin通tong過guo采cai用yong靜jing汞gong電dian極ji等deng一yi係xi列lie技ji術shu解jie決jue好hao這zhe個ge問wen題ti。在zai這zhe個ge技ji術shu領ling域yu是shi勝sheng過guo任ren何he一yi款kuan同tong類lei儀yi器qi,這zhe可ke通tong過guo現xian場chang比bi較jiao來lai證zheng實shi。另ling外wai一yi類lei電dian化hua學xue儀yi器qi則ze回hui避bi了le這zhe類lei問wen題ti,采cai用yong固gu體ti電dian極ji來lai測ce所suo有you元yuan素su,並bing從cong環huan保bao角jiao度du攻gong擊ji使shi用yong極ji譜pu方fang法fa的de儀yi器qi使shi用yong了le汞gong電dian極ji。其qi實shi在zai檢jian測ce中zhong,汞gong都dou在zai封feng閉bi環huan境jing中zhong工gong作zuo,不bu與yu大da氣qi接jie觸chu。就jiu如ru血xue壓ya計ji,目mu前qian的de測ce的de準zhun的de還hai是shi水shui銀yin血xue壓ya計ji,還hai在zai廣guang泛fan使shi用yong。使shi用yong滴di汞gong電dian極ji的de極ji譜pu分fen析xi方fang法fa,在zai很hen多duo領ling域yu裏li都dou是shi國guo標biao法fa和he行xing業ye標biao準zhun。例li如ru血xue清qing中zhong鋅xin測ce定ding是shi衛wei生sheng部bu檢jian驗yan規gui程cheng規gui定ding方fang法fa,而er食shi品pin中zhong極ji譜pu分fen析xi標biao準zhun更geng多duo。而er使shi用yong固gu體ti電dian極ji(如玻碳電極)測ce某mou些xie特te定ding元yuan素su如ru鉛qian效xiao果guo是shi好hao的de,但dan以yi不bu變bian應ying萬wan變bian用yong其qi來lai解jie決jue所suo有you元yuan素su的de檢jian測ce是shi不bu可ke能neng的de,無wu論lun是shi從cong理li論lun上shang還hai是shi實shi踐jian上shang都dou缺que少shao佐zuo證zheng。那na些xie花hua大da價jia錢qian買mai這zhe類lei儀yi器qi的de,要yao麼me就jiu是shi知zhi識shi不bu夠gou,要yao麼me是shi另ling有you原yuan因yin。微wei量liang元yuan素su分fen析xi因yin含han量liang低di,有you用yong信xin號hao小xiao,對dui技ji術shu要yao求qiu很hen高gao。做zuo的de好hao的de重zhong複fu性xing好hao,靈ling敏min度du高gao,儀yi器qi性xing能neng穩wen定ding,做zuo不bu好hao的de,重zhong複fu性xing差cha,整zheng個ge儀yi器qi基ji礎chu差cha,就jiu要yao用yong各ge種zhong手shou段duan應ying付fu用yong戶hu,隱yin瞞man真zhen相xiang,而er用yong戶hu對dui此ci知zhi之zhi甚shen少shao。最zui簡jian單dan判pan斷duan方fang法fa是shi看kan儀yi器qi是shi否fou設she置zhi了le能neng方fang便bian地di進jin行xing多duo條tiao曲qu線xian迭die加jia比bi較jiao、zhijieguanchazhongfuxinggongneng,nengfoufangbiandiqiubianyixishu。zaijinyibushiceyixiaxuezhongxin,duocijiancekanzhongfuxinghaohuai,yinxindehanliangjiaodi,nengkaoheyiqidexingneng,zuozhiqianxujianceyixiakongbai,fangzhishijikongbaiguogaozaochengjiaxiang。
zaizuohaozhongfuxingdejichushangcaiyoukenengkaochaqitaxingnengzhibiao,keguandeshuo,zhiyaozhongfuxingzuohaole,qitaxingnengzhibiaoyingwentibuda。danshinazhongyongyizhongdianjizuosuoyouyuansudeyiqi,zuokongbaijiabiaozhunrongyeheshiceyangpinyoutianrangzhibie。jiushishuoruguobuzuoyangpinzhizuodanchundebiaozhunrongye,kenenghenhao,danshijiaruyangpin,yangpindailaigezhongganraoshizhongfuxing、線性、靈敏度都有非常大的變化。目前使用固體玻炭電極測血鉛比較成熟。其他應看看國家、行xing業ye有you無wu這zhe方fang麵mian的de標biao準zhun,有you沒mei有you這zhe方fang麵mian的de文wen獻xian,有you文wen獻xian的de有you沒mei有you實shi際ji用yong於yu樣yang品pin的de範fan例li。如ru果guo都dou沒mei有you,有you的de企qi業ye卻que在zai很hen短duan的de時shi間jian內nei用yong這zhe種zhong電dian極ji搞gao出chu了le一yi套tao分fen析xi方fang法fa,究jiu竟jing是shi能neng力li超chao強qiang還hai是shi另ling有you原yuan因yin,就jiu需xu感gan興xing趣qu者zhe自zi己ji考kao慮lv了le。
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