1.分析天平在使用前沒有經過校準
一(yi)台(tai)分(fen)析(xi)天(tian)平(ping)在(zai)使(shi)用(yong)之(zhi)前(qian),首(shou)先(xian)要(yao)確(que)認(ren)它(ta)的(de)正(zheng)確(que)性(xing)是(shi)否(fou)合(he)格(ge),否(fou)則(ze)該(gai)天(tian)平(ping)所(suo)稱(cheng)量(liang)的(de)正(zheng)確(que)性(xing)得(de)不(bu)到(dao)保(bao)證(zheng)。分(fen)析(xi)天(tian)平(ping)從(cong)首(shou)次(ci)使(shi)用(yong)起(qi),應(ying)對(dui)其(qi)定(ding)期(qi)校(xiao)準(zhun)。連(lian)續(xu)使(shi)用(yong)的(de)天(tian)平(ping),大(da)約(yue)每(mei)星(xing)期(qi)校(xiao)準(zhun)一(yi)次(ci)。校(xiao)準(zhun)時(shi)應(ying)按(an)規(gui)定(ding)程(cheng)序(xu)進(jin)行(xing),必(bi)須(xu)使(shi)用(yong)標(biao)準(zhun)砝(fa)碼(ma)進(jin)行(xing)校(xiao)準(zhun),否(fou)則(ze)將(jiang)起(qi)不(bu)到(dao)校(xiao)準(zhun)的(de)作(zuo)用(yong)。
2.分析天平安裝不正確
在安裝分析天平時首先要選擇選防塵、防潮、防震、防風、防曬、hengwendefangjianzuoweitianpingshi。qici,tianpingyinganfangzailaogukekaodegongzuotaishang,bingxuanzeshidangdeweizhianfang。tianpinganzhuangqian,yinganzhuangxiangqingdanjinxingqingdian,kangebujianshifouqiquan、完(wan)好(hao),並(bing)對(dui)天(tian)平(ping)的(de)所(suo)有(you)部(bu)件(jian)進(jin)行(xing)仔(zai)細(xi)清(qing)潔(jie)。安(an)裝(zhuang)時(shi),應(ying)參(can)照(zhao)天(tian)平(ping)的(de)說(shuo)明(ming)書(shu)正(zheng)確(que)裝(zhuang)配(pei)天(tian)平(ping)。安(an)裝(zhuang)完(wan)畢(bi)後(hou)應(ying)再(zai)次(ci)檢(jian)查(zha)各(ge)部(bu)分(fen)安(an)裝(zhuang)是(shi)否(fou)正(zheng)常(chang),然(ran)後(hou)檢(jian)查(zha)電(dian)源(yuan)電(dian)壓(ya)是(shi)否(fou)符(fu)合(he)天(tian)平(ping)的(de)要(yao)求(qiu),打(da)開(kai)天(tian)平(ping)檢(jian)查(zha)是(shi)否(fou)正(zheng)常(chang)。
3.環境及樣品的物理因素影響
在使用分析天平進行稱量的過程中,環境和物理因素會對稱量結果產生幹擾,如溫度、樣品揮發、吸濕、磁力、靜電等的幹擾。
(1)溫度的變化對分析天平的影響
ruguozaichengliangguochengzhongfaxianxianshizhidanfangxiangpiaoyi,jiuyoukenengshiwendubianhuasuochanshengdeyingxiang。ruoyangpinyuzhouweihuanjingzhijiandewenducunzaichayi,zezhegewenduchayijiuhuidaozhiyanchengzhongrongqiliudongdeqiliu。kongqiyanzherongqiwaiceliudongchanshengyigexiangshangdezuoyongli,zhegelijiudaozhichengzhongjieguochanshengcuowu:樣(yang)品(pin)在(zai)動(dong)態(tai)浮(fu)力(li)作(zuo)用(yong)下(xia),稱(cheng)得(de)的(de)重(zhong)量(liang)比(bi)實(shi)際(ji)要(yao)輕(qing)。這(zhe)個(ge)作(zuo)用(yong)直(zhi)到(dao)溫(wen)度(du)平(ping)衡(heng)形(xing)成(cheng)以(yi)後(hou)才(cai)會(hui)終(zhong)止(zhi)。當(dang)把(ba)樣(yang)品(pin)從(cong)幹(gan)燥(zao)爐(lu)或(huo)冰(bing)箱(xiang)中(zhong)取(qu)出(chu)以(yi)後(hou),要(yao)等(deng)到(dao)樣(yang)品(pin)溫(wen)度(du)與(yu)實(shi)驗(yan)室(shi)或(huo)稱(cheng)量(liang)室(shi)溫(wen)度(du)一(yi)致(zhi)時(shi)才(cai)可(ke)以(yi)稱(cheng)量(liang)。樣(yang)品(pin)要(yao)放(fang)在(zai)表(biao)麵(mian)積(ji)盡(jin)可(ke)能(neng)小(xiao)的(de)去(qu)皮(pi)容(rong)器(qi)中(zhong),取(qu)放(fang)稱(cheng)量(liang)容(rong)器(qi)要(yao)使(shi)用(yong)鑷(nie)子(zi)夾(jia)取(qu),而(er)不(bu)能(neng)將(jiang)手(shou)放(fang)入(ru)稱(cheng)量(liang)室(shi)中(zhong)。
(2)樣品吸濕或揮發對稱量結果的影響
如果在稱量的過程中顯示值單方向持續漂移,則可能測量的是揮發性或吸濕性樣品。若樣品吸濕性較強,則重量會增大;若(ruo)被(bei)測(ce)量(liang)樣(yang)品(pin)屬(shu)易(yi)揮(hui)發(fa)物(wu)質(zhi),則(ze)重(zhong)量(liang)會(hui)減(jian)小(xiao)。對(dui)於(yu)吸(xi)濕(shi)性(xing)或(huo)揮(hui)發(fa)性(xing)樣(yang)品(pin)可(ke)使(shi)用(yong)細(xi)頸(jing)容(rong)器(qi),給(gei)容(rong)器(qi)加(jia)蓋(gai)或(huo)上(shang)塞(sai),使(shi)用(yong)清(qing)潔(jie)幹(gan)燥(zao)的(de)稱(cheng)重(zhong)容(rong)器(qi)並(bing)保(bao)持(chi)稱(cheng)盤(pan)上(shang)不(bu)粘(zhan)有(you)灰(hui)塵(chen)、汙染物及水滴。
(3)樣品或容器帶靜電對稱量結果的影響
如(ru)果(guo)每(mei)次(ci)稱(cheng)量(liang)都(dou)顯(xian)示(shi)不(bu)同(tong)的(de)稱(cheng)量(liang)結(jie)果(guo)或(huo)顯(xian)示(shi)值(zhi)不(bu)穩(wen)定(ding),或(huo)稱(cheng)量(liang)結(jie)果(guo)的(de)重(zhong)複(fu)性(xing)差(cha),則(ze)可(ke)考(kao)慮(lv)是(shi)稱(cheng)量(liang)容(rong)器(qi)或(huo)者(zhe)樣(yang)品(pin)帶(dai)有(you)靜(jing)電(dian)。靜(jing)電(dian)現(xian)象(xiang)的(de)影(ying)響(xiang)將(jiang)使(shi)每(mei)次(ci)稱(cheng)量(liang)時(shi)稱(cheng)重(zhong)容(rong)器(qi)均(jun)顯(xian)示(shi)不(bu)同(tong)的(de)重(zhong)量(liang),結(jie)果(guo)的(de)重(zhong)複(fu)性(xing)很(hen)差(cha)。具(ju)有(you)高(gao)絕(jue)緣(yuan)度(du)的(de)材(cai)料(liao)如(ru)玻(bo)璃(li)、塑su料liao製zhi的de稱cheng重zhong容rong器qi等deng容rong易yi帶dai靜jing電dian。這zhe種zhong帶dai電dian現xian象xiang主zhu要yao是shi由you於yu樣yang品pin或huo容rong器qi在zai搬ban運yun過guo程cheng中zhong攪jiao拌ban或huo摩mo擦ca產chan生sheng的de,而er且qie一yi旦dan帶dai電dian則ze排pai除chu電dian荷he會hui非fei常chang緩huan慢man,在zai相xiang對dui濕shi度du低di於yu40%的de幹gan燥zao空kong氣qi中zhong出chu現xian樣yang品pin或huo容rong器qi帶dai靜jing電dian的de幾ji率lv會hui增zeng加jia。通tong常chang可ke采cai用yong打da開kai加jia濕shi器qi或huo適shi當dang調tiao節jie空kong調tiao係xi統tong來lai增zeng加jia空kong氣qi濕shi度du,把ba稱cheng重zhong容rong器qi放fang在zai金jin屬shu容rong器qi內nei再zai進jin行xing稱cheng量liang,設she法fa給gei分fen析xi天tian平ping接jie地di等deng措cuo施shi,來lai去qu除chu或huo屏ping蔽bi稱cheng重zhong樣yang品pin上shang的de靜jing電dian。
4.使用者操作不當造成稱量不準確
稱量前沒有檢查,盲目稱量。稱量前應檢查天平是否正常,天平是否水平,稱盤是否潔淨、顯示屏是否歸零“000”位等等。
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