shiyanshideyiqishebeishiwomendegongzuodadang,lianghaodeshiyongheweihuxiguan,keyishiwomenshiyangengdexinyingshou,namejutizhexieshebeiyinggairuheweihune,yiqikan看吧。
電子天平
dianzitianpingshiwomendeshiyanzhongbibeidechenglianggongju,dabufenshiyanrenyuanyejibennengzhangwoqishiyongfangfa,danshiyandexijiehedasaoweihuzuodehenbudaowei,shiyanhouchengpanxiacanliuyouyixiewuzhi,chengpanshangliuyouwuzi。shitianpingdelingminduhezhunqueduxiajiang,shiyongshoumingyesuoduan。dianzitianpingshiyongqianxuxianyure10分鍾,但部分實驗人員開機後直接稱量。
稱(cheng)量(liang)物(wu)的(de)溫(wen)度(du)必(bi)須(xu)與(yu)天(tian)平(ping)溫(wen)度(du)相(xiang)同(tong),不(bu)能(neng)把(ba)過(guo)熱(re)或(huo)過(guo)冷(leng)的(de)物(wu)體(ti)放(fang)在(zai)天(tian)平(ping)秤(cheng)盤(pan)上(shang)。一(yi)些(xie)具(ju)有(you)揮(hui)發(fa)性(xing)的(de)腐(fu)蝕(shi)性(xing)的(de)試(shi)劑(ji)應(ying)放(fang)在(zai)密(mi)閉(bi)容(rong)器(qi)中(zhong)稱(cheng)量(liang),稱(cheng)量(liang)物(wu)體(ti)時(shi)要(yao)切(qie)記(ji)關(guan)閉(bi)天(tian)平(ping)的(de)側(ce)門(men),稱(cheng)量(liang)完(wan)畢(bi)後(hou)及(ji)時(shi)打(da)掃(sao)稱(cheng)量(liang)盤(pan)上(shang)下(xia)及(ji)各(ge)個(ge)角(jiao)落(luo)等(deng)。
在空氣潮濕,物質已結成垢塊時,應采用機械除鏽方法,即先用鏟、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。
電熱恒溫幹燥箱
電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100~110度(du),不(bu)宜(yi)過(guo)高(gao)。可(ke)燃(ran)性(xing)和(he)揮(hui)發(fa)性(xing)的(de)化(hua)學(xue)物(wu)品(pin)切(qie)勿(wu)放(fang)入(ru)箱(xiang)內(nei),箱(xiang)內(nei)載(zai)物(wu)應(ying)擺(bai)放(fang)應(ying)在(zai)隔(ge)板(ban)的(de)較(jiao)中(zhong)心(xin)部(bu)位(wei),同(tong)時(shi)不(bu)影(ying)響(xiang)空(kong)氣(qi)流(liu)通(tong)以(yi)保(bao)證(zheng)箱(xiang)內(nei)溫(wen)度(du)均(jun)勻(yun)。
幹燥箱使用過程中,學生不能用濕手觸摸箱體和開關。幹燥箱正常運行時如在使用過程中出現異常、氣味、煙(yan)霧(wu)等(deng)情(qing)況(kuang),應(ying)立(li)即(ji)關(guan)閉(bi)電(dian)源(yuan),請(qing)專(zhuan)業(ye)人(ren)員(yuan)查(zha)看(kan)修(xiu)理(li)。箱(xiang)壁(bi)內(nei)膽(dan)和(he)設(she)備(bei)表(biao)麵(mian)要(yao)經(jing)常(chang)擦(ca)拭(shi),以(yi)保(bao)持(chi)清(qing)潔(jie),增(zeng)加(jia)玻(bo)璃(li)的(de)透(tou)明(ming)度(du)。幹(gan)燥(zao)箱(xiang)若(ruo)長(chang)期(qi)不(bu)用(yong),應(ying)拔(ba)掉(diao)電(dian)源(yuan)線(xian)以(yi)防(fang)止(zhi)設(she)備(bei)損(sun)傷(shang)人(ren),並(bing)應(ying)定(ding)期(qi)按(an)使(shi)用(yong)條(tiao)件(jian)運(yun)行(xing)2~3天,以驅除電器部分的潮氣,避免損壞有關器件。
恒溫水浴鍋
恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、jiaoyukeyandebibeigongju。zaishiyongzhongxueshengyinggaizhidaotadeshiyongfangfajizhuyishixiang,yibianshiyannenggoushunlijinxing。jiashuizhiqianqiewujietongdianyuan,zuihaojiaruzhengliushui,yimianchanshengshuigou,jiashuibuyaotaiduo,yimianfeitengshishuiliangyichuguowai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;qiewuwushuihuoshuiweidiyugebanjiare,fouzehuisunhuaijiareguan。zhushuishibunengjiangshuiliurukongzhixiangnei,yifangfashengchudian。ruhengwenkongzhishiling,kejiangkongzhiqishangdeyinjiedianyongxishabucaliang。shiyongwanbihou,quchuhengwenwu,guanbidianyuan,paichuxiangtineideshui,zuohaoyiqishiyongjilu。
燒杯
燒杯因其口徑上下一致,是取用液體、配製溶液、做(zuo)簡(jian)單(dan)化(hua)學(xue)反(fan)應(ying)最(zui)常(chang)用(yong)的(de)反(fan)應(ying)容(rong)器(qi)。但(dan)燒(shao)杯(bei)不(bu)能(neng)代(dai)替(ti)量(liang)筒(tong)量(liang)取(qu)液(ye)體(ti)。燒(shao)杯(bei)加(jia)熱(re)時(shi)要(yao)墊(dian)上(shang)石(shi)棉(mian)網(wang)。不(bu)能(neng)用(yong)火(huo)焰(yan)直(zhi)接(jie)加(jia)熱(re)燒(shao)杯(bei)。因(yin)為(wei)燒(shao)杯(bei)底(di)麵(mian)大(da),用(yong)火(huo)焰(yan)直(zhi)接(jie)加(jia)熱(re),隻(zhi)可(ke)燒(shao)到(dao)局(ju)部(bu),使(shi)玻(bo)璃(li)受(shou)熱(re)不(bu)勻(yun)而(er)引(yin)起(qi)炸(zha)裂(lie)。用(yong)燒(shao)杯(bei)加(jia)熱(re)液(ye)體(ti)時(shi),液(ye)體(ti)的(de)量(liang)以(yi)不(bu)超(chao)過(guo)燒(shao)杯(bei)容(rong)積(ji)的(de)1/3為(wei)宜(yi),以(yi)防(fang)沸(fei)騰(teng)時(shi)液(ye)體(ti)外(wai)溢(yi)。加(jia)熱(re)時(shi),燒(shao)杯(bei)外(wai)壁(bi)須(xu)擦(ca)幹(gan)。加(jia)熱(re)腐(fu)蝕(shi)性(xing)藥(yao)品(pin)時(shi),可(ke)將(jiang)一(yi)表(biao)麵(mian)皿(min)蓋(gai)在(zai)燒(shao)杯(bei)口(kou)上(shang),以(yi)免(mian)液(ye)體(ti)濺(jian)出(chu)。不(bu)可(ke)用(yong)燒(shao)杯(bei)長(chang)期(qi)盛(sheng)放(fang)化(hua)學(xue)藥(yao)品(pin),以(yi)免(mian)落(luo)入(ru)塵(chen)土(tu)和(he)使(shi)溶(rong)液(ye)中(zhong)的(de)水(shui)分(fen)蒸(zheng)發(fa)。溶(rong)解(jie)或(huo)稀(xi)釋(shi)過(guo)程(cheng)中(zhong),用(yong)玻(bo)璃(li)棒(bang)攪(jiao)拌(ban)時(shi),不(bu)要(yao)觸(chu)及(ji)杯(bei)底(di)或(huo)杯(bei)壁(bi)。
試管
實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。加jia熱re時shi要yao保bao持chi試shi管guan外wai壁bi沒mei有you水shui珠zhu,防fang止zhi受shou熱re不bu均jun勻yun而er爆bao裂lie。加jia熱re後hou不bu能neng驟zhou冷leng,防fang止zhi試shi管guan破po裂lie。加jia熱re後hou不bu能neng在zai試shi管guan未wei冷leng卻que至zhi室shi溫wen時shi就jiu洗xi滌di試shi管guan。加jia熱re時shi應ying用yong外wai焰yan。
容量瓶
容(rong)量(liang)瓶(ping)主(zhu)要(yao)用(yong)於(yu)準(zhun)確(que)地(di)配(pei)製(zhi)一(yi)定(ding)摩(mo)爾(er)濃(nong)度(du)的(de)溶(rong)液(ye),它(ta)是(shi)一(yi)種(zhong)細(xi)長(chang)頸(jing),梨(li)形(xing)的(de)平(ping)底(di)玻(bo)璃(li)瓶(ping),帶(dai)有(you)磨(mo)口(kou)玻(bo)璃(li)塞(sai),瓶(ping)頸(jing)上(shang)刻(ke)有(you)標(biao)線(xian),當(dang)瓶(ping)內(nei)液(ye)體(ti)在(zai)所(suo)指(zhi)定(ding)溫(wen)度(du)下(xia)達(da)到(dao)標(biao)線(xian)處(chu)時(shi),其(qi)體(ti)積(ji)即(ji)為(wei)瓶(ping)上(shang)所(suo)注(zhu)明(ming)的(de)容(rong)積(ji)數(shu)。
容(rong)量(liang)瓶(ping)不(bu)能(neng)配(pei)製(zhi)其(qi)容(rong)積(ji)以(yi)下(xia)體(ti)積(ji)的(de)溶(rong)液(ye),即(ji)其(qi)容(rong)積(ji)為(wei)多(duo)大(da),就(jiu)隻(zhi)能(neng)配(pei)製(zhi)多(duo)大(da)體(ti)積(ji)的(de)溶(rong)液(ye)。容(rong)量(liang)瓶(ping)使(shi)用(yong)前(qian)應(ying)先(xian)檢(jian)查(zha)是(shi)否(fou)漏(lou)水(shui),依(yi)次(ci)用(yong)自(zi)來(lai)水(shui),蒸(zheng)餾(liu)水(shui)洗(xi)好(hao)備(bei)用(yong)。將(jiang)溶(rong)質(zhi)在(zai)燒(shao)杯(bei)中(zhong)溶(rong)解(jie)後(hou)轉(zhuan)移(yi)到(dao)容(rong)量(liang)瓶(ping)裏(li),不(bu)能(neng)在(zai)容(rong)量(liang)瓶(ping)裏(li)進(jin)行(xing)溶(rong)質(zhi)的(de)溶(rong)解(jie),控(kong)製(zhi)溶(rong)解(jie)溶(rong)質(zhi)的(de)蒸(zheng)餾(liu)水(shui)量(liang)。
轉zhuan移yi時shi必bi須xu用yong玻bo璃li棒bang引yin流liu。容rong量liang瓶ping不bu能neng進jin行xing加jia熱re,如ru果guo溶rong質zhi在zai溶rong解jie過guo程cheng中zhong放fang熱re,要yao待dai溶rong液ye冷leng卻que後hou再zai進jin行xing轉zhuan移yi,因yin為wei溫wen度du升sheng高gao瓶ping體ti將jiang膨peng脹zhang,所suo量liang體ti積ji就jiu會hui不bu準zhun確que。用yong於yu洗xi滌di燒shao杯bei的de溶rong劑ji總zong量liang不bu能neng超chao過guo容rong量liang瓶ping的de標biao線xian,一yi旦dan超chao過guo,必bi須xu重zhong新xin進jin行xing配pei置zhi。
配(pei)製(zhi)好(hao)的(de)溶(rong)液(ye)轉(zhuan)移(yi)至(zhi)試(shi)劑(ji)瓶(ping)中(zhong)保(bao)存(cun),容(rong)量(liang)瓶(ping)隻(zhi)能(neng)配(pei)製(zhi)溶(rong)液(ye),不(bu)能(neng)儲(chu)存(cun)溶(rong)液(ye),因(yin)為(wei)溶(rong)液(ye)可(ke)能(neng)會(hui)對(dui)瓶(ping)體(ti)進(jin)行(xing)腐(fu)蝕(shi),從(cong)而(er)使(shi)容(rong)量(liang)瓶(ping)的(de)精(jing)度(du)受(shou)到(dao)影(ying)響(xiang)。容(rong)量(liang)瓶(ping)使(shi)用(yong)完(wan)畢(bi)應(ying)及(ji)時(shi)用(yong)水(shui)衝(chong)洗(xi)幹(gan)淨(jing),塞(sai)上(shang)瓶(ping)塞(sai),並(bing)在(zai)塞(sai)子(zi)與(yu)瓶(ping)口(kou)之(zhi)間(jian)夾(jia)一(yi)條(tiao)紙(zhi)條(tiao),防(fang)止(zhi)瓶(ping)塞(sai)與(yu)瓶(ping)口(kou)粘(zhan)連(lian)。最(zui)後(hou)記(ji)錄(lu)溶(rong)液(ye)體(ti)積(ji)的(de)時(shi)候(hou)一(yi)般(ban)保(bao)留(liu)4位有效數字(XXX.0mL)。
滴定管
滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水依次衝洗幹淨,並要用待裝的溶液潤洗滴定管。
將jiang操cao作zuo溶rong液ye倒dao入ru,直zhi到dao充chong滿man至zhi零ling刻ke度du線xian以yi上shang為wei止zhi。注zhu意yi檢jian查zha滴di定ding管guan的de出chu口kou管guan是shi否fou充chong滿man溶rong液ye,如ru有you氣qi泡pao進jin行xing排pai氣qi泡pao操cao作zuo。調tiao整zheng液ye麵mian時shi,使shi液ye麵mian保bao持chi在zai“0”或“0”以(yi)下(xia)的(de)某(mou)一(yi)定(ding)刻(ke)度(du)。進(jin)行(xing)滴(di)定(ding)時(shi),應(ying)將(jiang)滴(di)定(ding)管(guan)垂(chui)直(zhi)地(di)夾(jia)在(zai)滴(di)定(ding)管(guan)夾(jia)上(shang),如(ru)使(shi)用(yong)的(de)是(shi)堿(jian)式(shi)滴(di)定(ding)管(guan),拇(mu)指(zhi)與(yu)食(shi)指(zhi)在(zai)玻(bo)璃(li)珠(zhu)所(suo)在(zai)部(bu)位(wei)一(yi)旁(pang)捏(nie)乳(ru)膠(jiao)管(guan),不(bu)要(yao)捏(nie)玻(bo)璃(li)珠(zhu),也(ye)不(bu)能(neng)使(shi)其(qi)上(shang)下(xia)移(yi)動(dong)。滴(di)定(ding)時(shi)應(ying)逐(zhu)滴(di)連(lian)續(xu)滴(di)加(jia),接(jie)近(jin)終(zhong)點(dian)時(shi),隻(zhi)加(jia)一(yi)滴(di)或(huo)半(ban)滴(di),至(zhi)溶(rong)液(ye)出(chu)現(xian)明(ming)顯(xian)的(de)顏(yan)色(se)變(bian)化(hua)。
讀數時,手拿滴定管上部無刻度處,使滴定管保持垂直,視線平視溶液的凹液麵,讀到小數點後第二位,即估計到0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
常用玻璃儀器的洗滌
實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。
附fu有you易yi去qu除chu物wu質zhi的de簡jian單dan儀yi器qi,如ru試shi管guan。燒shao杯bei等deng,先xian用yong自zi來lai水shui衝chong洗xi,再zai用yong試shi管guan刷shua蘸zhan取qu合he成cheng洗xi滌di劑ji刷shua洗xi,最zui後hou自zi來lai水shui衝chong洗xi。當dang倒dao置zhi儀yi器qi,器qi壁bi形xing成cheng一yi層ceng均jun勻yun的de水shui膜mo,不bu成cheng股gu流liu下xia時shi,即ji已yi洗xi淨jing。有you油you汙wu的de玻bo璃li器qi皿min,先xian用yong堿jian性xing酒jiu精jing洗xi滌di液ye洗xi滌di,然ran後hou用yong洗xi衣yi粉fen水shui或huo肥fei皂zao水shui洗xi滌di,再zai用yong自zi來lai水shui衝chong洗xi幹gan淨jing。有you鏽xiu跡ji,水shui垢gou的de器qi皿min,用yong(1+3)yansuanxiyejinpao,zaiyongzailaishuichongxiganjing。youfanshilinyouwudeqimin,xianjiangfanshilincaqu,zaiyongxiyifenshuihuofeizaoshuixishaozhu,quchuhouyongzilaishuichongxiganjing。yixiegouzaobijiaojingxi、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。
常用光學儀器的維護與清洗
實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、pengzhuangyiqi,yifangzhiguangxuelingjiansunshangjiyingxiangjingdu。beiceshiyangzhongbuyingyouyingxingzazhi,dangceshigutishiyangshi,yingfangzhibazheshelengjingbiaomianlamaohuochanshengyahen。shiyongwanbihou,yanjinzhijiefangrushuizhongqingxi,bimianguangxuexitongguanlujinshui。dakailengjing,yongcajingzhiqingqingcagan,bulunzairenheqingkuangxia,buyunxuyongcajingzhiyiwaiderenhedongxijiechudaolengjing,yimiansunhuaitadeguangxuepingmian。yiqiyingcunfangyuganzao、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、顯(xian)微(wei)鏡(jing)的(de)鏡(jing)頭(tou),先(xian)用(yong)蒸(zheng)餾(liu)水(shui)進(jin)行(xing)清(qing)洗(xi),鏡(jing)麵(mian)若(ruo)有(you)汙(wu)漬(zi),可(ke)以(yi)用(yong)乙(yi)醇(chun)和(he)乙(yi)醚(mi)的(de)混(hun)合(he)液(ye)清(qing)洗(xi)。清(qing)洗(xi)時(shi)用(yong)專(zhuan)門(men)的(de)擦(ca)鏡(jing)紙(zhi)或(huo)棉(mian)球(qiu)沾(zhan)有(you)少(shao)量(liang)清(qing)洗(xi)劑(ji),順(shun)著(zhe)一(yi)個(ge)方(fang)向(xiang)擦(ca)拭(shi),從(cong)鏡(jing)頭(tou)中(zhong)心(xin)向(xiang)外(wai)作(zuo)圓(yuan)運(yun)動(dong),切(qie)忌(ji)把(ba)這(zhe)類(lei)鏡(jing)頭(tou)浸(jin)泡(pao)在(zai)清(qing)洗(xi)劑(ji)中(zhong)清(qing)洗(xi)。清(qing)洗(xi)鏡(jing)頭(tou)不(bu)得(de)用(yong)力(li)拭(shi)擦(ca),否(fou)則(ze)會(hui)劃(hua)傷(shang)增(zeng)透(tou)膜(mo),損(sun)壞(huai)鏡(jing)頭(tou)。清(qing)洗(xi)完(wan)畢(bi)後(hou)用(yong)擦(ca)鏡(jing)紙(zhi)擦(ca)幹(gan),避(bi)光(guang)保(bao)存(cun)。
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