1. 分析天平在使用前沒有經過校準
一yi台tai分fen析xi天tian平ping在zai使shi用yong之zhi前qian,首shou先xian要yao確que認ren它ta的de正zheng確que性xing是shi否fou合he格ge,否fou則ze該gai天tian平ping所suo稱cheng量liang的de正zheng確que性xing得de不bu到dao保bao證zheng。分fen析xi天tian平ping從cong首shou次ci使shi用yong起qi,應ying對dui其qi定ding期qi校xiao準zhun。連lian續xu使shi用yong的de天tian平ping,大da約yue每mei星xing期qi校xiao準zhun一yi次ci。校xiao準zhun時shi應ying按an規gui定ding程cheng序xu進jin行xing,必bi須xu使shi用yong標biao準zhun砝fa碼ma進jin行xing校xiao準zhun,否fou則ze將jiang起qi不bu到dao校xiao準zhun的de作zuo用yong。
2. 分析天平安裝不正確
在安裝分析天平時首先要選擇選防塵、防潮、防震、防風、防曬、hengwendefangjianzuoweitianpingshi。qici,tianpingyinganfangzailaogukekaodegongzuotaishang,bingxuanzeshidangdeweizhianfang。tianpinganzhuangqian,yinganzhuangxiangqingdanjinxingqingdian,kangebujianshifouqiquan、wanhao,bingduitianpingdesuoyoubujianjinxingzaixiqingjie。anzhuangshi,yingcanzhaotianpingdeshuomingshuzhengquezhuangpeitianping。anzhuangwanbihouyingzaicijianzhagebufenanzhuangshifouzhengchang,ranhoujianzhadianyuandianyashifoufuhetianpingdeyaoqiu,dakaitianpingjianzhashifouzhengchang。
3. 環境及樣品的物理因素影響
在使用分析天平進行稱量的過程中,環境和物理因素會對稱量結果產生幹擾,如溫度、樣品揮發、吸濕、磁力、靜電等的幹擾。
(1)溫度的變化對分析天平的影響
如(ru)果(guo)在(zai)稱(cheng)量(liang)過(guo)程(cheng)中(zhong)發(fa)現(xian)顯(xian)示(shi)值(zhi)單(dan)方(fang)向(xiang)漂(piao)移(yi),就(jiu)有(you)可(ke)能(neng)是(shi)溫(wen)度(du)變(bian)化(hua)所(suo)產(chan)生(sheng)的(de)影(ying)響(xiang)。若(ruo)樣(yang)品(pin)與(yu)周(zhou)圍(wei)環(huan)境(jing)之(zhi)間(jian)的(de)溫(wen)度(du)存(cun)在(zai)差(cha)異(yi),則(ze)這(zhe)個(ge)溫(wen)度(du)差(cha)異(yi)就(jiu)會(hui)導(dao)致(zhi)沿(yan)稱(cheng)重(zhong)容(rong)器(qi)流(liu)動(dong)的(de)氣(qi)流(liu)。空(kong)氣(qi)沿(yan)著(zhe)容(rong)器(qi)外(wai)側(ce)流(liu)動(dong)產(chan)生(sheng)一(yi)個(ge)向(xiang)上(shang)的(de)作(zuo)用(yong)力(li),這(zhe)個(ge)力(li)就(jiu)導(dao)致(zhi)稱(cheng)重(zhong)結(jie)果(guo)產(chan)生(sheng)錯(cuo)誤(wu):樣(yang)品(pin)在(zai)動(dong)態(tai)浮(fu)力(li)作(zuo)用(yong)下(xia),稱(cheng)得(de)的(de)重(zhong)量(liang)比(bi)實(shi)際(ji)要(yao)輕(qing)。這(zhe)個(ge)作(zuo)用(yong)直(zhi)到(dao)溫(wen)度(du)平(ping)衡(heng)形(xing)成(cheng)以(yi)後(hou)才(cai)會(hui)終(zhong)止(zhi)。當(dang)把(ba)樣(yang)品(pin)從(cong)幹(gan)燥(zao)爐(lu)或(huo)冰(bing)箱(xiang)中(zhong)取(qu)出(chu)以(yi)後(hou),要(yao)等(deng)到(dao)樣(yang)品(pin)溫(wen)度(du)與(yu)實(shi)驗(yan)室(shi)或(huo)稱(cheng)量(liang)室(shi)溫(wen)度(du)一(yi)致(zhi)時(shi)才(cai)可(ke)以(yi)稱(cheng)量(liang)。樣(yang)品(pin)要(yao)放(fang)在(zai)表(biao)麵(mian)積(ji)盡(jin)可(ke)能(neng)小(xiao)的(de)去(qu)皮(pi)容(rong)器(qi)中(zhong),取(qu)放(fang)稱(cheng)量(liang)容(rong)器(qi)要(yao)使(shi)用(yong)鑷(nie)子(zi)夾(jia)取(qu),而(er)不(bu)能(neng)將(jiang)手(shou)放(fang)入(ru)稱(cheng)量(liang)室(shi)中(zhong)。
(2)樣品吸濕或揮發對稱量結果的影響
如果在稱量的過程中顯示值單方向持續漂移,則可能測量的是揮發性或吸濕性樣品。若樣品吸濕性較強,則重量會增大;若ruo被bei測ce量liang樣yang品pin屬shu易yi揮hui發fa物wu質zhi,則ze重zhong量liang會hui減jian小xiao。對dui於yu吸xi濕shi性xing或huo揮hui發fa性xing樣yang品pin可ke使shi用yong細xi頸jing容rong器qi,給gei容rong器qi加jia蓋gai或huo上shang塞sai,使shi用yong清qing潔jie幹gan燥zao的de稱cheng重zhong容rong器qi並bing保bao持chi稱cheng盤pan上shang不bu粘zhan有you灰hui塵chen、汙染物及水滴。
(3)樣品或容器帶靜電對稱量結果的影響
ruguomeicichengliangdouxianshibutongdechengliangjieguohuoxianshizhibuwending,huochengliangjieguodezhongfuxingcha,zekekaolvshichengliangrongqihuozheyangpindaiyoujingdian。jingdianxianxiangdeyingxiangjiangshimeicichengliangshichengzhongrongqijunxianshibutongdezhongliang,jieguodezhongfuxinghencha。juyougaojueyuandudecailiaoruboli、suliaozhidechengzhongrongqidengrongyidaijingdian。zhezhongdaidianxianxiangzhuyaoshiyouyuyangpinhuorongqizaibanyunguochengzhongjiaobanhuomocachanshengde,erqieyidandaidianzepaichudianhehuifeichanghuanman,zaixiangduishidudiyu40%的(de)幹(gan)燥(zao)空(kong)氣(qi)中(zhong)出(chu)現(xian)樣(yang)品(pin)或(huo)容(rong)器(qi)帶(dai)靜(jing)電(dian)的(de)幾(ji)率(lv)會(hui)增(zeng)加(jia)。通(tong)常(chang)可(ke)采(cai)用(yong)打(da)開(kai)加(jia)濕(shi)器(qi)或(huo)適(shi)當(dang)調(tiao)節(jie)空(kong)調(tiao)係(xi)統(tong)來(lai)增(zeng)加(jia)空(kong)氣(qi)濕(shi)度(du),把(ba)稱(cheng)重(zhong)容(rong)器(qi)放(fang)在(zai)金(jin)屬(shu)容(rong)器(qi)內(nei)再(zai)進(jin)行(xing)稱(cheng)量(liang),設(she)法(fa)給(gei)分(fen)析(xi)天(tian)平(ping)接(jie)地(di)等(deng)措(cuo)施(shi),來(lai)去(qu)除(chu)或(huo)屏(ping)蔽(bi)稱(cheng)重(zhong)樣(yang)品(pin)上(shang)的(de)靜(jing)電(dian)。
4.使用者操作不當造成稱量不準確
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