(1)電子天平
電dian子zi天tian平ping是shi我wo們men的de化hua學xue實shi驗yan中zhong必bi備bei的de稱cheng量liang工gong具ju,學xue生sheng也ye基ji本ben能neng掌zhang握wo其qi使shi用yong方fang法fa,但dan實shi驗yan的de細xi節jie和he打da掃sao維wei護hu做zuo的de很hen不bu到dao位wei,實shi驗yan後hou秤cheng盤pan下xia殘can留liu有you一yi些xie物wu質zhi,秤cheng盤pan上shang留liu有you汙wu漬zi。使shi天tian平ping的de靈ling敏min度du和he準zhun確que度du下xia降jiang,使shi用yong壽shou命ming也ye縮suo短duan。電dian子zi天tian平ping使shi用yong前qian須xu先xian預yu熱re10分(fen)鍾(zhong),但(dan)部(bu)分(fen)學(xue)生(sheng)開(kai)機(ji)後(hou)直(zhi)接(jie)稱(cheng)量(liang)。稱(cheng)量(liang)物(wu)的(de)溫(wen)度(du)必(bi)須(xu)與(yu)天(tian)平(ping)溫(wen)度(du)相(xiang)同(tong),不(bu)能(neng)把(ba)過(guo)熱(re)或(huo)過(guo)冷(leng)的(de)物(wu)體(ti)放(fang)在(zai)天(tian)平(ping)秤(cheng)盤(pan)上(shang)。一(yi)些(xie)具(ju)有(you)揮(hui)發(fa)性(xing)的(de)腐(fu)蝕(shi)性(xing)的(de)試(shi)劑(ji)應(ying)放(fang)在(zai)密(mi)閉(bi)容(rong)器(qi)中(zhong)稱(cheng)量(liang),稱(cheng)量(liang)物(wu)體(ti)時(shi)要(yao)切(qie)記(ji)關(guan)閉(bi)天(tian)平(ping)的(de)側(ce)門(men),稱(cheng)量(liang)完(wan)畢(bi)後(hou)及(ji)時(shi)打(da)掃(sao)稱(cheng)量(liang)盤(pan)上(shang)下(xia)及(ji)各(ge)個(ge)角(jiao)落(luo)等(deng)。在(zai)空(kong)氣(qi)潮(chao)濕(shi),物(wu)質(zhi)已(yi)結(jie)成(cheng)垢(gou)塊(kuai)時(shi),應(ying)采(cai)用(yong)機(ji)械(xie)除(chu)鏽(xiu)方(fang)法(fa),即(ji)先(xian)用(yong)鏟(chan)、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。
(2)電熱恒溫幹燥箱
電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100-110度(du),不(bu)宜(yi)過(guo)高(gao)。可(ke)燃(ran)性(xing)和(he)揮(hui)發(fa)性(xing)的(de)化(hua)學(xue)物(wu)品(pin)切(qie)勿(wu)放(fang)入(ru)箱(xiang)內(nei),箱(xiang)內(nei)載(zai)物(wu)應(ying)擺(bai)放(fang)應(ying)在(zai)隔(ge)板(ban)的(de)較(jiao)中(zhong)心(xin)部(bu)位(wei),同(tong)時(shi)不(bu)影(ying)響(xiang)空(kong)氣(qi)流(liu)通(tong)以(yi)保(bao)證(zheng)箱(xiang)內(nei)溫(wen)度(du)均(jun)勻(yun)。幹(gan)燥(zao)箱(xiang)使(shi)用(yong)過(guo)程(cheng)中(zhong),學(xue)生(sheng)不(bu)能(neng)用(yong)濕(shi)手(shou)觸(chu)摸(mo)箱(xiang)體(ti)和(he)開(kai)關(guan)。幹(gan)燥(zao)箱(xiang)正(zheng)常(chang)運(yun)行(xing)時(shi)如(ru)在(zai)使(shi)用(yong)過(guo)程(cheng)中(zhong)出(chu)現(xian)異(yi)常(chang)、氣味、煙(yan)霧(wu)等(deng)情(qing)況(kuang),應(ying)立(li)即(ji)關(guan)閉(bi)電(dian)源(yuan),請(qing)專(zhuan)業(ye)人(ren)員(yuan)查(zha)看(kan)修(xiu)理(li)。箱(xiang)壁(bi)內(nei)膽(dan)和(he)設(she)備(bei)表(biao)麵(mian)要(yao)經(jing)常(chang)擦(ca)拭(shi),以(yi)保(bao)持(chi)清(qing)潔(jie),增(zeng)加(jia)玻(bo)璃(li)的(de)透(tou)明(ming)度(du)。幹(gan)燥(zao)箱(xiang)若(ruo)長(chang)期(qi)不(bu)用(yong),應(ying)拔(ba)掉(diao)電(dian)源(yuan)線(xian)以(yi)防(fang)止(zhi)設(she)備(bei)損(sun)傷(shang)人(ren),並(bing)應(ying)定(ding)期(qi)按(an)使(shi)用(yong)條(tiao)件(jian)運(yun)行(xing)2-3天,以驅除電器部分的潮氣,避免損壞有關器件。
(3)恒溫水浴鍋
恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、jiaoyukeyandebibeigongju。zaishiyongzhongxueshengyinggaizhidaotadeshiyongfangfajizhuyishixiang,yibianshiyannenggoushunlijinxing。jiashuizhiqianqiewujietongdianyuan,zuihaojiaruzhengliushui,yimianchanshengshuigou,jiashuibuyaotaiduo,yimianfeitengshishuiliangyichuguowai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;qiewuwushuihuoshuiweidiyugebanjiare,fouzehuisunhuaijiareguan。zhushuishibunengjiangshuiliurukongzhixiangnei,yifangfashengchudian。ruhengwenkongzhishiling,kejiangkongzhiqishangdeyinjiedianyongxishabucaliang。shiyongwanbihou,quchuhengwenwu,guanbidianyuan,paichuxiangtineideshui,zuohaoyiqishiyongjilu。
(1)燒杯
燒杯因其口徑上下一致,是取用液體、配製溶液、zuojiandanhuaxuefanyingzuichangyongdefanyingrongqi。danshaobeibunengdaitiliangtongliangquyeti。shaobeijiareshiyaodianshangshimianwang。bunengyonghuoyanzhijiejiareshaobei。yinweishaobeidimianda,yonghuoyanzhijiejiare,zhikeshaodaojubu,shibolishourebuyuneryinqizhalie。yongshaobeijiareyetishi,yetideliangyibuchaoguoshaobeirongjide1/3為wei宜yi,以yi防fang沸fei騰teng時shi液ye體ti外wai溢yi。加jia熱re時shi,燒shao杯bei外wai壁bi須xu擦ca幹gan。加jia熱re腐fu蝕shi性xing藥yao品pin時shi,可ke將jiang一yi表biao麵mian皿min蓋gai在zai燒shao杯bei口kou上shang,以yi免mian液ye體ti濺jian出chu。不bu可ke用yong燒shao杯bei長chang期qi盛sheng放fang化hua學xue藥yao品pin,以yi免mian落luo入ru塵chen土tu和he使shi溶rong液ye中zhong的de水shui分fen蒸zheng發fa。溶rong解jie或huo稀xi釋shi過guo程cheng中zhong,用yong玻bo璃li棒bang攪jiao拌ban時shi,不bu要yao觸chu及ji杯bei底di或huo杯bei壁bi。
(2)試管
實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。加jia熱re時shi要yao保bao持chi試shi管guan外wai壁bi沒mei有you水shui珠zhu,防fang止zhi受shou熱re不bu均jun勻yun而er爆bao裂lie。加jia熱re後hou不bu能neng驟zhou冷leng,防fang止zhi試shi管guan破po裂lie。加jia熱re後hou不bu能neng在zai試shi管guan未wei冷leng卻que至zhi室shi溫wen時shi就jiu洗xi滌di試shi管guan。加jia熱re時shi應ying用yong外wai焰yan。
(3)容量瓶
rongliangpingzhuyaoyongyuzhunquedipeizhiyidingmoernongduderongye,tashiyizhongxichangjing,lixingdepingdiboliping,daiyoumokoubolisai,pingjingshangkeyoubiaoxian,dangpingneiyetizaisuozhidingwenduxiadadaobiaoxianchushi,qitijijiweipingshangsuozhumingderongjishu。rongliangpingbunengpeizhiqirongjiyixiatijiderongye,jiqirongjiweiduoda,jiuzhinengpeizhiduodatijiderongye。rongliangpingshiyongqianyingxianjianzhashifouloushui,yiciyongzilaishui,zhengliushuixihaobeiyong。jiangrongzhizaishaobeizhongrongjiehouzhuanyidaorongliangpingli,bunengzairongliangpinglijinxingrongzhiderongjie,kongzhirongjierongzhidezhengliushuiliang。zhuanyishibixuyongbolibangyinliu。rongliangpingbunengjinxingjiare,ruguorongzhizairongjieguochengzhongfangre,yaodairongyelengquehouzaijinxingzhuanyi,yinweiwendushenggaopingtijiangpengzhang,suoliangtijijiuhuibuzhunque。yongyuxidishaobeiderongjizongliangbunengchaoguorongliangpingdebiaoxian,yidanchaoguo,bixuzhongxinjinxingpeizhi。peizhihaoderongyezhuanyizhishijipingzhongbaocun,rongliangpingzhinengpeizhirongye,bunengchucunrongye,yinweirongyekenenghuiduipingtijinxingfushi,congershirongliangpingdejingdushoudaoyingxiang。rongliangpingshiyongwanbiyingjishiyongshuichongxiganjing,saishangpingsai,bingzaisaiziyupingkouzhijianjiayitiaozhitiao,fangzhipingsaiyupingkouzhanlian。zuihoujilurongyetijideshihouyibanbaoliu4位有效數字(XXX.0mL)。
(4)滴定管
滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、shuiyicichongxiganjing,bingyaoyongdaizhuangderongyerunxididingguan。jiangcaozuorongyedaoru,zhidaochongmanzhilingkeduxianyishangweizhi。zhuyijianzhadidingguandechukouguanshifouchongmanrongye,ruyouqipaojinxingpaiqipaocaozuo。tiaozhengyemianshi,shiyemianbaochizai“0”或“0”以(yi)下(xia)的(de)某(mou)一(yi)定(ding)刻(ke)度(du)。進(jin)行(xing)滴(di)定(ding)時(shi),應(ying)將(jiang)滴(di)定(ding)管(guan)垂(chui)直(zhi)地(di)夾(jia)在(zai)滴(di)定(ding)管(guan)夾(jia)上(shang),如(ru)使(shi)用(yong)的(de)是(shi)堿(jian)式(shi)滴(di)定(ding)管(guan),拇(mu)指(zhi)與(yu)食(shi)指(zhi)在(zai)玻(bo)璃(li)珠(zhu)所(suo)在(zai)部(bu)位(wei)一(yi)旁(pang)捏(nie)乳(ru)膠(jiao)管(guan),不(bu)要(yao)捏(nie)玻(bo)璃(li)珠(zhu),也(ye)不(bu)能(neng)使(shi)其(qi)上(shang)下(xia)移(yi)動(dong)。滴(di)定(ding)時(shi)應(ying)逐(zhu)滴(di)連(lian)續(xu)滴(di)加(jia),接(jie)近(jin)終(zhong)點(dian)時(shi),隻(zhi)加(jia)一(yi)滴(di)或(huo)半(ban)滴(di),至(zhi)溶(rong)液(ye)出(chu)現(xian)明(ming)顯(xian)的(de)顏(yan)色(se)變(bian)化(hua)。讀(du)數(shu)時(shi),手(shou)拿(na)滴(di)定(ding)管(guan)上(shang)部(bu)無(wu)刻(ke)度(du)處(chu),使(shi)滴(di)定(ding)管(guan)保(bao)持(chi)垂(chui)直(zhi),視(shi)線(xian)平(ping)視(shi)溶(rong)液(ye)的(de)凹(ao)液(ye)麵(mian),讀(du)到(dao)小(xiao)數(shu)點(dian)後(hou)第(di)二(er)位(wei),即(ji)估(gu)計(ji)到(dao)0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。
實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。
fuyouyiquchuwuzhidejiandanyiqi,rushiguan。shaobeideng,xianyongzilaishuichongxi,zaiyongshiguanshuazhanquhechengxidijishuaxi,zuihouzilaishuichongxi。dangdaozhiyiqi,qibixingchengyicengjunyundeshuimo,buchengguliuxiashi,jiyixijing。
有油汙的玻璃器皿,先用堿性酒精洗滌液洗滌,然後用洗衣粉水或肥皂水洗滌,再用自來水衝洗幹淨。
有鏽跡,水垢的器皿,用(1+3)鹽酸洗液浸泡,再用再來水衝洗幹淨。
有凡士林油汙的器皿,先將凡士林擦去,再用洗衣粉水或肥皂水洗燒煮,取出後用自來水衝洗幹淨。
一些構造比較精細、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。
洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。
實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、碰(peng)撞(zhuang)儀(yi)器(qi),以(yi)防(fang)止(zhi)光(guang)學(xue)零(ling)件(jian)損(sun)傷(shang)及(ji)影(ying)響(xiang)精(jing)度(du)。被(bei)測(ce)試(shi)樣(yang)中(zhong)不(bu)應(ying)有(you)硬(ying)性(xing)雜(za)質(zhi),當(dang)測(ce)試(shi)固(gu)體(ti)試(shi)樣(yang)時(shi),應(ying)防(fang)止(zhi)把(ba)折(zhe)射(she)棱(leng)鏡(jing)表(biao)麵(mian)拉(la)毛(mao)或(huo)產(chan)生(sheng)壓(ya)痕(hen)。使(shi)用(yong)完(wan)畢(bi)後(hou),嚴(yan)禁(jin)直(zhi)接(jie)放(fang)入(ru)水(shui)中(zhong)清(qing)洗(xi),避(bi)免(mian)光(guang)學(xue)係(xi)統(tong)管(guan)路(lu)進(jin)水(shui)。打(da)開(kai)棱(leng)鏡(jing),用(yong)擦(ca)鏡(jing)紙(zhi)輕(qing)輕(qing)擦(ca)幹(gan),不(bu)論(lun)在(zai)任(ren)何(he)情(qing)況(kuang)下(xia),不(bu)允(yun)許(xu)用(yong)擦(ca)鏡(jing)紙(zhi)以(yi)外(wai)的(de)任(ren)何(he)東(dong)西(xi)接(jie)觸(chu)到(dao)棱(leng)鏡(jing),以(yi)免(mian)損(sun)壞(huai)它(ta)的(de)光(guang)學(xue)平(ping)麵(mian)。儀(yi)器(qi)應(ying)存(cun)放(fang)於(yu)幹(gan)燥(zao)、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。
光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、顯(xian)微(wei)鏡(jing)的(de)鏡(jing)頭(tou),先(xian)用(yong)蒸(zheng)餾(liu)水(shui)進(jin)行(xing)清(qing)洗(xi),鏡(jing)麵(mian)若(ruo)有(you)汙(wu)漬(zi),可(ke)以(yi)用(yong)乙(yi)醇(chun)和(he)乙(yi)醚(mi)的(de)混(hun)合(he)液(ye)清(qing)洗(xi)。清(qing)洗(xi)時(shi)用(yong)專(zhuan)門(men)的(de)擦(ca)鏡(jing)紙(zhi)或(huo)棉(mian)球(qiu)沾(zhan)有(you)少(shao)量(liang)清(qing)洗(xi)劑(ji),順(shun)著(zhe)一(yi)個(ge)方(fang)向(xiang)擦(ca)拭(shi),從(cong)鏡(jing)頭(tou)中(zhong)心(xin)向(xiang)外(wai)作(zuo)圓(yuan)運(yun)動(dong),切(qie)忌(ji)把(ba)這(zhe)類(lei)鏡(jing)頭(tou)浸(jin)泡(pao)在(zai)清(qing)洗(xi)劑(ji)中(zhong)清(qing)洗(xi)。清(qing)洗(xi)鏡(jing)頭(tou)不(bu)得(de)用(yong)力(li)拭(shi)擦(ca),否(fou)則(ze)會(hui)劃(hua)傷(shang)增(zeng)透(tou)膜(mo),損(sun)壞(huai)鏡(jing)頭(tou)。清(qing)洗(xi)完(wan)畢(bi)後(hou)用(yong)擦(ca)鏡(jing)紙(zhi)擦(ca)幹(gan),避(bi)光(guang)保(bao)存(cun)。
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