【幹貨】常用儀器的維護與清洗方法彙總

發布日期:2024-04-09
核心提示: 實驗室的儀器設備是我們的工作搭檔,良好的使用和維護習慣,可以使我們實驗更得心應手,那麼具體這些設備應該如何維護呢,
實shi驗yan室shi的de儀yi器qi設she備bei是shi我wo們men的de工gong作zuo搭da檔dang,良liang好hao的de使shi用yong和he維wei護hu習xi慣guan,可ke以yi使shi我wo們men實shi驗yan更geng得de心xin應ying手shou,那na麼me具ju體ti這zhe些xie設she備bei應ying該gai如ru何he維wei護hu呢ne,一yi起qi跟gen小xiao編bian來lai看kan看kan吧ba。dianzitianpingshiwomendeshiyanzhongbibeidechenglianggongju,dabufenshiyanrenyuanyejibennengzhangwoqishiyongfangfa,danshiyandexijiehedasaoweihuzuodehenbudaowei,shiyanhouchengpanxiacanliuyouyixiewuzhi,chengpanshangliuyouwuzi。shitianpingdelingminduhezhunqueduxiajiang,shiyongshoumingyesuoduan。dianzitianpingshiyongqianxuxianyure10分鍾,但部分實驗人員開機後直接稱量。稱cheng量liang物wu的de溫wen度du必bi須xu與yu天tian平ping溫wen度du相xiang同tong,不bu能neng把ba過guo熱re或huo過guo冷leng的de物wu體ti放fang在zai天tian平ping秤cheng盤pan上shang。一yi些xie具ju有you揮hui發fa性xing的de腐fu蝕shi性xing的de試shi劑ji應ying放fang在zai密mi閉bi容rong器qi中zhong稱cheng量liang,稱cheng量liang物wu體ti時shi要yao切qie記ji關guan閉bi天tian平ping的de側ce門men,稱cheng量liang完wan畢bi後hou及ji時shi打da掃sao稱cheng量liang盤pan上shang下xia及ji各ge個ge角jiao落luo等deng。在空氣潮濕,物質已結成垢塊時,應采用機械除鏽方法,即先用鏟、剔、刮等方式將零部件上的鏽蝕層塊除去,再用砂紙砂磨、打光,最後塗上保護層。實驗完畢,關閉側門,蓋上天平布,置於避光幹燥處保存。電熱恒溫幹燥箱是化學實驗中用於對物品進行烘焙、幹燥的常規儀器。幹燥箱的工作電壓為220V,溫度為100~110度,不宜過高。可燃性和揮發性的化學物品切勿放入箱內,箱內載物應擺放應在隔板的較中心部位,同時不影響空氣流通以保證箱內溫度均勻。幹燥箱使用過程中,學生不能用濕手觸摸箱體和開關。幹燥箱正常運行時如在使用過程中出現異常、氣味、煙(yan)霧(wu)等(deng)情(qing)況(kuang),應(ying)立(li)即(ji)關(guan)閉(bi)電(dian)源(yuan),請(qing)專(zhuan)業(ye)人(ren)員(yuan)查(zha)看(kan)修(xiu)理(li)。箱(xiang)壁(bi)內(nei)膽(dan)和(he)設(she)備(bei)表(biao)麵(mian)要(yao)經(jing)常(chang)擦(ca)拭(shi),以(yi)保(bao)持(chi)清(qing)潔(jie),增(zeng)加(jia)玻(bo)璃(li)的(de)透(tou)明(ming)度(du)。幹(gan)燥(zao)箱(xiang)若(ruo)長(chang)期(qi)不(bu)用(yong),應(ying)拔(ba)掉(diao)電(dian)源(yuan)線(xian)以(yi)防(fang)止(zhi)設(she)備(bei)損(sun)傷(shang)人(ren),並(bing)應(ying)定(ding)期(qi)按(an)使(shi)用(yong)條(tiao)件(jian)運(yun)行(xing)2~3天,以驅除電器部分的潮氣,避免損壞有關器件。恒溫水浴鍋主要用於實驗室中蒸餾,幹燥,濃縮化學藥品,也可用於恒溫加熱和其它溫度試驗,是化學實驗室、分析室、教育科研的必備工具。zaishiyongzhongxueshengyinggaizhidaotadeshiyongfangfajizhuyishixiang,yibianshiyannenggoushunlijinxing。jiashuizhiqianqiewujietongdianyuan,zuihaojiaruzhengliushui,yimianchanshengshuigou,jiashuibuyaotaiduo,yimianfeitengshishuiliangyichuguowai;鍋內水量也不可低於二分之一,不能使加熱管露出水麵;切勿無水或水位低於隔板加熱,否則會損壞加熱管。注zhu水shui時shi不bu能neng將jiang水shui流liu入ru控kong製zhi箱xiang內nei,以yi防fang發fa生sheng觸chu電dian。如ru恒heng溫wen控kong製zhi失shi靈ling,可ke將jiang控kong製zhi器qi上shang的de銀yin接jie點dian用yong細xi砂sha布bu擦ca亮liang。使shi用yong完wan畢bi後hou,取qu出chu恒heng溫wen物wu,關guan閉bi電dian源yuan,排pai除chu箱xiang體ti內nei的de水shui,做zuo好hao儀yi器qi使shi用yong記ji錄lu。燒杯因其口徑上下一致,是取用液體、配製溶液、做簡單化學反應最常用的反應容器。但燒杯不能代替量筒量取液體。燒杯加熱時要墊上石棉網。不能用火焰直接加熱燒杯。因為燒杯底麵大,用火焰直接加熱,隻可燒到局部,使玻璃受熱不勻而引起炸裂。用燒杯加熱液體時,液體的量以不超過燒杯容積的1/3為宜,以防沸騰時液體外溢。jiareshi,shaobeiwaibixucagan。jiarefushixingyaopinshi,kejiangyibiaomianmingaizaishaobeikoushang,yimianyetijianchu。bukeyongshaobeichangqishengfanghuaxueyaopin,yimianluoruchentuheshirongyezhongdeshuifenzhengfa。rongjiehuoxishiguochengzhong,yongbolibangjiaobanshi,buyaochujibeidihuobeibi。實驗室用來盛放少量藥品,加熱情況下少量試劑反應的容器。裝溶液時不超過試管容量的1/2,加熱時不超過試管的1/3。取塊狀固體放入試管要用鑷子,不能使固體直接墜入試管中,防止試管底破裂。加熱時使用試管夾,試管夾應夾在距管口1/3處。試管口不能對著人。試管不可以直接加熱,要先預熱,加熱盛有固體的試管時,管口略向下,加熱液體時傾斜約45°。jiareshiyaobaochishiguanwaibimeiyoushuizhu,fangzhishourebujunyunerbaolie。jiarehoubunengzhouleng,fangzhishiguanpolie。jiarehoubunengzaishiguanweilengquezhishiwenshijiuxidishiguan。jiareshiyingyongwaiyan。容量瓶主要用於準確地配製一定摩爾濃度derongye,tashiyizhongxichangjing,lixingdepingdiboliping,daiyoumokoubolisai,pingjingshangkeyoubiaoxian,dangpingneiyetizaisuozhidingwenduxiadadaobiaoxianchushi,qitijijiweipingshangsuozhumingderongjishu。容(rong)量(liang)瓶(ping)不(bu)能(neng)配(pei)製(zhi)其(qi)容(rong)積(ji)以(yi)下(xia)體(ti)積(ji)的(de)溶(rong)液(ye),即(ji)其(qi)容(rong)積(ji)為(wei)多(duo)大(da),就(jiu)隻(zhi)能(neng)配(pei)製(zhi)多(duo)大(da)體(ti)積(ji)的(de)溶(rong)液(ye)。容(rong)量(liang)瓶(ping)使(shi)用(yong)前(qian)應(ying)先(xian)檢(jian)查(zha)是(shi)否(fou)漏(lou)水(shui),依(yi)次(ci)用(yong)自(zi)來(lai)水(shui),蒸(zheng)餾(liu)水(shui)洗(xi)好(hao)備(bei)用(yong)。將(jiang)溶(rong)質(zhi)在(zai)燒(shao)杯(bei)中(zhong)溶(rong)解(jie)後(hou)轉(zhuan)移(yi)到(dao)容(rong)量(liang)瓶(ping)裏(li),不(bu)能(neng)在(zai)容(rong)量(liang)瓶(ping)裏(li)進(jin)行(xing)溶(rong)質(zhi)的(de)溶(rong)解(jie),控(kong)製(zhi)溶(rong)解(jie)溶(rong)質(zhi)的(de)蒸(zheng)餾(liu)水(shui)量(liang)。轉(zhuan)移(yi)時(shi)必(bi)須(xu)用(yong)玻(bo)璃(li)棒(bang)引(yin)流(liu)。容(rong)量(liang)瓶(ping)不(bu)能(neng)進(jin)行(xing)加(jia)熱(re),如(ru)果(guo)溶(rong)質(zhi)在(zai)溶(rong)解(jie)過(guo)程(cheng)中(zhong)放(fang)熱(re),要(yao)待(dai)溶(rong)液(ye)冷(leng)卻(que)後(hou)再(zai)進(jin)行(xing)轉(zhuan)移(yi),因(yin)為(wei)溫(wen)度(du)升(sheng)高(gao)瓶(ping)體(ti)將(jiang)膨(peng)脹(zhang),所(suo)量(liang)體(ti)積(ji)就(jiu)會(hui)不(bu)準(zhun)確(que)。用(yong)於(yu)洗(xi)滌(di)燒(shao)杯(bei)的(de)溶(rong)劑(ji)總(zong)量(liang)不(bu)能(neng)超(chao)過(guo)容(rong)量(liang)瓶(ping)的(de)標(biao)線(xian),一(yi)旦(dan)超(chao)過(guo),必(bi)須(xu)重(zhong)新(xin)進(jin)行(xing)配(pei)置(zhi)。配pei製zhi好hao的de溶rong液ye轉zhuan移yi至zhi試shi劑ji瓶ping中zhong保bao存cun,容rong量liang瓶ping隻zhi能neng配pei製zhi溶rong液ye,不bu能neng儲chu存cun溶rong液ye,因yin為wei溶rong液ye可ke能neng會hui對dui瓶ping體ti進jin行xing腐fu蝕shi,從cong而er使shi容rong量liang瓶ping的de精jing度du受shou到dao影ying響xiang。容rong量liang瓶ping使shi用yong完wan畢bi應ying及ji時shi用yong水shui衝chong洗xi幹gan淨jing,塞sai上shang瓶ping塞sai,並bing在zai塞sai子zi與yu瓶ping口kou之zhi間jian夾jia一yi條tiao紙zhi條tiao,防fang止zhi瓶ping塞sai與yu瓶ping口kou粘zhan連lian。最zui後hou記ji錄lu溶rong液ye體ti積ji的de時shi候hou一yi般ban保bao留liu4位有效數字(XXX.0mL)。滴定管是可放出不固定量液體的量出式玻璃儀器,主要用於滴定分析中對滴定劑體積的測量。能精確到到0.01mL。帶玻璃活塞的滴定管為酸式滴定管,帶有內裝玻璃球的橡皮管的滴定管為堿式滴定管。酸式、堿式滴定管不能混用,酸式滴定管裝酸性物質和大多數中性物質(尤其是強氧化劑),堿式滴定管裝堿性物質(包括堿和堿性鹽),滴定管使用前先檢查是否漏液,如果漏水,應重新將活塞塗凡士林油。裝液前要用洗液、水依次衝洗幹淨,並要用待裝的溶液潤洗滴定管。將(jiang)操(cao)作(zuo)溶(rong)液(ye)倒(dao)入(ru),直(zhi)到(dao)充(chong)滿(man)至(zhi)零(ling)刻(ke)度(du)線(xian)以(yi)上(shang)為(wei)止(zhi)。注(zhu)意(yi)檢(jian)查(zha)滴(di)定(ding)管(guan)的(de)出(chu)口(kou)管(guan)是(shi)否(fou)充(chong)滿(man)溶(rong)液(ye),如(ru)有(you)氣(qi)泡(pao)進(jin)行(xing)排(pai)氣(qi)泡(pao)操(cao)作(zuo)。調(tiao)整(zheng)液(ye)麵(mian)時(shi),使(shi)液(ye)麵(mian)保(bao)持(chi)在(zai)“0”或“0”以下的某一定刻度。進行滴定時,應將滴定管垂直地夾在滴定管夾上,如使用的是堿式滴定管,拇指與食指在玻璃珠所在部位一旁捏乳膠管,不要捏玻璃珠,也不能使其上下移動。滴定時應逐滴連續滴加,接近終點時,隻加一滴或半滴,至溶液出現明顯的顏色變化。讀數時,手拿滴定管上部無刻度處,使滴定管保持垂直,視線平視溶液的凹液麵,讀到小數點後第二位,即估計到0.01mL。滴定結束後,管內剩餘的溶液應棄去,不得將其倒回原瓶,隨即清洗滴定管,並倒掛於鐵架台上。 實驗室常用的玻璃儀器如燒杯、試管、滴定管、移液管、容量瓶等。儀器在使用中會沾上油汙,水垢,鏽跡等,使用後不及時完全的清洗,會造成結果誤差,甚至會對儀器的壽命、性能會產生極其不良的影響。因此,化學實驗使用的玻璃儀器必須洗滌幹淨。下麵介紹一些玻璃儀器的洗滌方法。fuyouyiquchuwuzhidejiandanyiqi,rushiguan。shaobeideng,xianyongzilaishuichongxi,zaiyongshiguanshuazhanquhechengxidijishuaxi,zuihouzilaishuichongxi。dangdaozhiyiqi,qibixingchengyicengjunyundeshuimo,buchengguliuxiashi,jiyixijing。youyouwudeboliqimin,xianyongjianxingjiujingxidiyexidi,ranhouyongxiyifenshuihuofeizaoshuixidi,zaiyongzilaishuichongxiganjing。youxiuji,shuigoudeqimin,yong(1+3)鹽yan酸suan洗xi液ye浸jin泡pao,再zai用yong再zai來lai水shui衝chong洗xi幹gan淨jing。有you凡fan士shi林lin油you汙wu的de器qi皿min,先xian將jiang凡fan士shi林lin擦ca去qu,再zai用yong洗xi衣yi粉fen水shui或huo肥fei皂zao水shui洗xi燒shao煮zhu,取qu出chu後hou用yong自zi來lai水shui衝chong洗xi幹gan淨jing。一yi些xie構gou造zao比bi較jiao精jing細xi、複雜的玻璃儀器,如容量瓶、移液管等,無法用毛刷刷洗,可以用洗滌液浸泡一定時間,再進行清洗。洗淨的玻璃儀器不要再用手、布或紙擦拭,以免重新汙染。實驗室常用的光學儀器如分光光度計、折光計的棱鏡、玻片等,都是一些精密光學儀器,在使用和保養中,必須細心謹慎,嚴格按說明使用,不得任意鬆動儀器各連接部分,不得跌落、碰撞儀器,以防止光學零件損傷及影響精度。被(bei)測(ce)試(shi)樣(yang)中(zhong)不(bu)應(ying)有(you)硬(ying)性(xing)雜(za)質(zhi),當(dang)測(ce)試(shi)固(gu)體(ti)試(shi)樣(yang)時(shi),應(ying)防(fang)止(zhi)把(ba)折(zhe)射(she)棱(leng)鏡(jing)表(biao)麵(mian)拉(la)毛(mao)或(huo)產(chan)生(sheng)壓(ya)痕(hen)。使(shi)用(yong)完(wan)畢(bi)後(hou),嚴(yan)禁(jin)直(zhi)接(jie)放(fang)入(ru)水(shui)中(zhong)清(qing)洗(xi),避(bi)免(mian)光(guang)學(xue)係(xi)統(tong)管(guan)路(lu)進(jin)水(shui)。打(da)開(kai)棱(leng)鏡(jing),用(yong)擦(ca)鏡(jing)紙(zhi)輕(qing)輕(qing)擦(ca)幹(gan),不(bu)論(lun)在(zai)任(ren)何(he)情(qing)況(kuang)下(xia),不(bu)允(yun)許(xu)用(yong)擦(ca)鏡(jing)紙(zhi)以(yi)外(wai)的(de)任(ren)何(he)東(dong)西(xi)接(jie)觸(chu)到(dao)棱(leng)鏡(jing),以(yi)免(mian)損(sun)壞(huai)它(ta)的(de)光(guang)學(xue)平(ping)麵(mian)。儀器應存放於幹燥、無灰塵、無油汙和無有害、易燃、易爆等氣體的地方,以免光學零件腐蝕或生黴。光學儀器在使用中容易沾上油汙、水濕性汙物、指紋等,影響成像及透光率。清洗折光計的棱鏡、平麵鏡、顯微鏡的鏡頭,先用蒸餾水進行清洗,鏡麵若有汙漬,可以用乙醇和乙醚的混合液清洗。清(qing)洗(xi)時(shi)用(yong)專(zhuan)門(men)的(de)擦(ca)鏡(jing)紙(zhi)或(huo)棉(mian)球(qiu)沾(zhan)有(you)少(shao)量(liang)清(qing)洗(xi)劑(ji),順(shun)著(zhe)一(yi)個(ge)方(fang)向(xiang)擦(ca)拭(shi),從(cong)鏡(jing)頭(tou)中(zhong)心(xin)向(xiang)外(wai)作(zuo)圓(yuan)運(yun)動(dong),切(qie)忌(ji)把(ba)這(zhe)類(lei)鏡(jing)頭(tou)浸(jin)泡(pao)在(zai)清(qing)洗(xi)劑(ji)中(zhong)清(qing)洗(xi)。清(qing)洗(xi)鏡(jing)頭(tou)不(bu)得(de)用(yong)力(li)拭(shi)擦(ca),否(fou)則(ze)會(hui)劃(hua)傷(shang)增(zeng)透(tou)膜(mo),損(sun)壞(huai)鏡(jing)頭(tou)。清(qing)洗(xi)完(wan)畢(bi)後(hou)用(yong)擦(ca)鏡(jing)紙(zhi)擦(ca)幹(gan),避(bi)光(guang)保(bao)存(cun)。
編輯:songjiajie2010